3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde

Base Information

• Chemical Name: 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde
• CAS No.: 1415935-04-4
• Molecular Formula: C₂₀H₁₈BClF₂N₂O
• Molecular Weight: 386.637

Synonyms:3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde

Chemical Property of 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde

Chemical Property:

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Technology Process of 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde

There total 1 articles about 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ⁴,6λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY (1355953-59-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ4,6λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde (1415935-04-4)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; at 20 ℃; for 0.583333h; Inert atmosphere; Cooling with ice;

3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY; In 1,2-dichloro-ethane; at 50 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2ob26791h

Reference yield: 89.0%

propylamine (107-10-8,42939-71-9) + 3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ4,6λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde (1415935-04-4) → 8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-3-(propylamino)-5H-5λ4,6λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde (1415935-02-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 4h;

DOI:10.1039/c2ob26791h

Reference yield: 84.0%

3-chloro-8-ethyl-5,5-difluoro-7,9-dimethyl-10-phenyl-5H-5λ4,6λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine-2-carbaldehyde (1415935-04-4) + para-thiocresol (106-45-6) → C27H25BF2N2OS

Guidance literature:

With dmap; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201712528

upstream raw materials:

3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY

N,N-dimethyl-formamide

Downstream raw materials:

C₂₇H₂₈BF₂N₃O₂

C₂₈H₃₁BF₂N₄O₂

C₂₉H₃₄BF₂N₅O₃

C₂₈H₃₀BF₂N₃O₃

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