3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY

Base Information

• Chemical Name: 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY
• CAS No.: 1355953-59-1
• Molecular Formula: C₁₉H₁₈BClF₂N₂
• Molecular Weight: 358.626
• Mol file: 1355953-59-1.mol

Synonyms:3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY

Chemical Property of 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY

There total 12 articles about 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

ClC4H3NCC6H5C4N(CH3)2CH2CH3 (1355953-56-8) + boron trifluoride diethyl etherate (109-63-7) → 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY (1355953-59-1)

Guidance literature:

ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃; With triethylamine; In toluene; at 20 ℃; for 1h;

boron trifluoride diethyl etherate; In toluene; at 0 - 105 ℃; for 3h;

DOI:10.1039/d0ob00082e

Reference yield:

2,4-dimethyl-3-ethyl-pyrrole (517-22-6) → 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY (1355953-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate

2: boron trifluoride diethyl etherate; triethylamine / toluene

With boron trifluoride diethyl etherate; triethylamine; trichlorophosphate; In toluene;

DOI:10.1016/j.dyepig.2012.08.026

Reference yield:

2-benzoyl-5-chloropyrrole (142231-06-9) → 3-chloro-5,7-dimethyl-6-ethyl-8-phenyl-BODIPY (1355953-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate

2: boron trifluoride diethyl etherate; triethylamine / toluene

With boron trifluoride diethyl etherate; triethylamine; trichlorophosphate; In toluene;

DOI:10.1016/j.dyepig.2012.08.026

upstream raw materials:

2,4-dimethyl-3-ethyl-pyrrole

2-benzoyl-5-chloropyrrole

ClC₄H₃NCC₆H₅C₄N(CH₃)2CH₂CH₃

boron trifluoride diethyl etherate

Downstream raw materials:

3-(4-methylphenyl)sulfinyl-5,7-dimethyl-6-ethyl-8-phenyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-(4-methylphenyl)sulfenyl-5,7-dimethyl-6-ethyl-8-phenyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-benzylsulfanyl-5,7-dimethyl-6-ethyl-8-phenyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-benzylsulfinyl-5,7-dimethyl-6-ethyl-8-phenyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene