C₂₀H₂₂INO₂S

Base Information

Chemical Name:C₂₀H₂₂INO₂S
CAS No.:1287656-32-9
Molecular Formula:C₂₀H₂₂INO₂S
Molecular Weight:467.371
Hs Code.:

C<sub>20</sub>H<sub>22</sub>INO<sub>2</sub>S

Synonyms:C₂₀H₂₂INO₂S

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Chemical Property of C₂₀H₂₂INO₂S

Chemical Property:

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Technology Process of C₂₀H₂₂INO₂S

There total 4 articles about C₂₀H₂₂INO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1287656-11-4
(Z)-N-(3-iodo-2-phenylallyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

: 1287656-32-9
C₂₀H₂₂INO₂S

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In toluene; at 120 ℃; for 16h; stereospecific reaction; Inert atmosphere;
DOI:10.1021/ja201204g

Reference yield:

: 3-iodo-2-phenyl-2-propen-1-ol

: 1287656-32-9
C₂₀H₂₂INO₂S

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 80 °C

3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; di-isopropyl azodicarboxylate; palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1021/ja201204g

Reference yield:

: 1287655-99-5
C₁₆H₁₆INO₂S

: 1287656-32-9
C₂₀H₂₂INO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 80 °C

2: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja201204g