4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

Base Information

Chemical Name:4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile
CAS No.:1426332-61-7
Molecular Formula:C₂₂H₁₄N₄O
Molecular Weight:350.379
Hs Code.:

Synonyms:4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

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Chemical Property of 4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

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Technology Process of 4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

There total 1 articles about 4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 31643-49-9
4-Nitrophthalonitrile

: 41097-41-0
2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenol

: 1426332-61-7
4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 55 ℃; for 120h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.saa.2012.12.058

Reference yield:

: 1426332-61-7
4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

: 1426332-62-8
C₈₈H₅₈N₁₆O₄

: C₈₈H₅₈N₁₆O₄

: C₈₈H₅₈N₁₆O₄

: C₈₈H₅₈N₁₆O₄

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 150 ℃; for 24h; Overall yield = 22 %; Overall yield = 46 mg; Sealed tube; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.saa.2012.12.058

Reference yield:

: 1426332-61-7
4-(2-{(E)-[(2E)-(phenylmethylidene)hydrazono]methyl}phenoxy)phthalonitrile

: 83864-14-6
nickel dichloride

: C₈₈H₅₆N₁₆NiO₄

: C₈₈H₅₆N₁₆NiO₄

: C₈₈H₅₆N₁₆NiO₄

: C₈₈H₅₆N₁₆NiO₄

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 150 ℃; for 24h; Overall yield = 28 %; Overall yield = 26 mg; Sealed tube; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.saa.2012.12.058