6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Base Information

Chemical Name:6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine
CAS No.:1318988-81-6
Molecular Formula:C₁₆H₉Cl₂N₃O₂S₄
Molecular Weight:474.436
Hs Code.:

Synonyms:6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Suppliers and Price of 6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

There total 3 articles about 6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1318988-76-9
4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

: 1318988-81-6
6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: With Lawessons reagent; In toluene; at 20 ℃; for 20h; Reflux;
DOI:10.3987/COM-11-12164

Reference yield:

: 156775-41-6
chlorek kwasu 6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksylowego

: 1318988-81-6
6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 5 - 20 °C

2: Lawessons reagent / toluene / 20 h / 20 °C / Reflux

With Lawessons reagent; In toluene; benzene;
DOI:10.3987/COM-11-12164

Reference yield:

: 6-chloro-3-(methylthio)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylic acid

: 1318988-81-6
6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride

2: benzene / 5 - 20 °C

3: Lawessons reagent / toluene / 20 h / 20 °C / Reflux

With Lawessons reagent; thionyl chloride; In toluene; benzene;
DOI:10.3987/COM-11-12164