4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Base Information

• Chemical Name: 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide
• CAS No.: 1318988-76-9
• Molecular Formula: C₁₆H₁₁Cl₂N₃O₄S₃
• Molecular Weight: 476.385

Synonyms:4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Chemical Property of 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

There total 2 articles about 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-chlorobenzoic acid hydrazide (536-40-3) + chlorek kwasu 6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksylowego (156775-41-6) → 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-76-9)

Guidance literature:

In benzene; at 5 - 20 ℃;

DOI:10.3987/COM-11-12164

Reference yield:

6-chloro-3-(methylthio)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylic acid → 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-76-9)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / benzene / Reflux

2: benzene / 5 - 20 °C

With thionyl chloride; In benzene;

DOI:10.3390/molecules201219821

Reference yield: 87.0%

4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-76-9) → 6-chloro-7-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine (1318988-79-2)

Guidance literature:

With thionyl chloride; at 20 ℃; for 21h; Reflux;

DOI:10.3987/COM-11-12164

upstream raw materials:

4-chlorobenzoic acid hydrazide

chlorek kwasu 6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksylowego

Downstream raw materials:

6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

3-amino-6-chloro-7-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

3-amino-6-chloro-7-[5-(4-chlorophenyl)-1,3,4-thiadiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

3-amino-2-{2-benzylthio-4-chloro-5-[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]benzenesulfonyl}guanidine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1318988-76-9 4-chloro-N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Send

Send

Metric Ton KG G Pound L ML

Send

Send