octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

Base Information

Chemical Name:octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside
CAS No.:459170-27-5
Molecular Formula:C₃₅H₃₉NO₇Se
Molecular Weight:664.657
Hs Code.:

Synonyms:octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

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Technology Process of octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

There total 2 articles about octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 645-96-5
Benzeneselenol

: 459170-60-6
Benzoic acid (2S,3S,4R,5R,6R)-2-bromomethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-4-hydroxy-6-octyloxy-tetrahydro-pyran-3-yl ester

: 459170-27-5
octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

Guidance literature:: With triethylamine; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/ja0127234

Reference yield:

: 161664-93-3
octyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 459170-27-5
octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

Guidance literature:: Multi-step reaction with 2 steps

1: NBS; BaCO₃ / CCl₄ / 1.25 h / Heating

2: 1.11 mg / Et₃N / tetrahydrofuran / 12 h / Heating

With N-Bromosuccinimide; triethylamine; barium carbonate; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/ja0127234

Reference yield: 81.0%

: 3587-60-8
Benzyloxymethyl chloride

: 459170-27-5
octyl 4-O-benzoyl-2,6-dideoxy-6-phenylseleno-2-phthalimido-β-D-glucopyraniside

: 1169770-87-9
4-O-benzoyl-2-phthalimido-2,6-dideoxy-3-O-[(benzyloxy)methyl]-6-phenylseleno-octyl-β-D-glucopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 71h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.03.025