6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

Base Information

Chemical Name:6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose
CAS No.:100740-75-8
Molecular Formula:C53H42 O10
Molecular Weight:838.89
Hs Code.:
Mol file:100740-75-8.mol

Synonyms:6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

Suppliers and Price of 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2,3,4-TETRA-O-BENZOYL-6-O-TRITYL-BETA-D-GALACTOPYRANOSE 95.00%
5MG
$ 504.66

Total 6 raw suppliers

Chemical Property of 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

Chemical Property:

Boiling Point:890.2±65.0 °C(Predicted)
PSA：123.66000
Density:1.33±0.1 g/cm3(Predicted)
LogP:9.25380

Purity/Quality:

98%min ^*data from raw suppliers

1,2,3,4-TETRA-O-BENZOYL-6-O-TRITYL-BETA-D-GALACTOPYRANOSE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

There total 1 articles about 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.8%

: 67919-33-9,160712-27-6,67919-34-0
6-O-trityl-D-galactose

: 98-88-4
benzoyl chloride

: 100740-74-7
1,2,3,4-tetra-O-benzoyl-6-O-trityl-α-D-galactopyranose

: 100740-75-8
1,2,3,4-tetra-O-benzoyl-6-O-trityl-β-D-galactopyranose

Guidance literature:: In pyridine; 1.) -60 deg C; 2.) RT, 3 h; 3.) 60 deg C, overnight;
DOI:10.1016/0008-6215(85)85130-2

Reference yield: 93.0%

: 100740-75-8
1,2,3,4-tetra-O-benzoyl-6-O-trityl-β-D-galactopyranose

: 100740-76-9
1,2,3,4-tetra-O-benzoyl-β-D-galactopyranose

Guidance literature:: With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 0 ℃; for 0.05h;
DOI:10.1016/0008-6215(85)85130-2

Reference yield:

: 100740-75-8
1,2,3,4-tetra-O-benzoyl-6-O-trityl-β-D-galactopyranose

: 100776-43-0
2,3,4-tri-O-benzoyl-6-O-bromoacetyl-α-D-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / NaI, (CH₃)3SiCl / acetonitrile / 0.05 h / 0 °C

2: 92 percent / 2,6-lutidine / CH₂Cl₂ / 0.17 h / -30 °C

3: 98 percent / HBr / acetic acid; CH₂Cl₂ / 0.67 h / Ambient temperature

With 2,6-dimethylpyridine; chloro-trimethyl-silane; hydrogen bromide; sodium iodide; In dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/0008-6215(85)85130-2