(Z)-3,4,5-trimethoxy-β-iodostyrene

Base Information

Chemical Name:(Z)-3,4,5-trimethoxy-β-iodostyrene
CAS No.:1388628-51-0
Molecular Formula:C₁₁H₁₃IO₃
Molecular Weight:320.127
Hs Code.:

Synonyms:(Z)-3,4,5-trimethoxy-β-iodostyrene

Suppliers and Price of (Z)-3,4,5-trimethoxy-β-iodostyrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-3,4,5-trimethoxy-β-iodostyrene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-3,4,5-trimethoxy-β-iodostyrene

There total 2 articles about (Z)-3,4,5-trimethoxy-β-iodostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 3020-28-8
(iodomethyl)triphenylphosphonium iodide

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1388628-51-0
(Z)-3,4,5-trimethoxy-β-iodostyrene

Guidance literature:: (iodomethyl)triphenylphosphonium iodide; With sodium hexamethyldisilazane; In tetrahydrofuran; at -20 ℃; for 0.25h;

3,4,5-trimethoxy-benzaldehyde; In tetrahydrofuran; at -78 ℃; for 2h; enantioselective reaction;
DOI:10.1016/j.bmc.2020.115684

Reference yield:

: iodomethylenetriphenylphosphonium iodide

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1388628-51-0
(Z)-3,4,5-trimethoxy-β-iodostyrene

: (E)-5-(2-Iodovinyl)-1,2,3-trimethoxybenzene

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - -20 ℃; for 3.25h; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0031-1290899

Reference yield: 84.0%

: 1388628-51-0
(Z)-3,4,5-trimethoxy-β-iodostyrene

: 87199-17-5
4-formylphenylboronic acid,

: 4-formyl-3′,4′,5′-trimethoxy-(Z)-stilbene

Guidance literature:: (Z)-3,4,5-trimethoxy-β-iodostyrene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; for 0.333333h; Inert atmosphere;

4-formylphenylboronic acid,; With sodium carbonate; In 1,2-dimethoxyethane; water; at 80 ℃; for 20h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.bmc.2020.115684