C₂₆H₁₄F₁₀N₂O

Base Information

Chemical Name:C₂₆H₁₄F₁₀N₂O
CAS No.:1346641-89-1
Molecular Formula:C₂₆H₁₄F₁₀N₂O
Molecular Weight:560.394
Hs Code.:

C<sub>26</sub>H<sub>14</sub>F<sub>10</sub>N<sub>2</sub>O

Synonyms:C₂₆H₁₄F₁₀N₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₁₄F₁₀N₂O

Chemical Property:

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Technology Process of C₂₆H₁₄F₁₀N₂O

There total 6 articles about C₂₆H₁₄F₁₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1346640-97-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methylcyclopropanecarboxamide

: 214360-65-3
4-trifluoromethylphenylboronic acid pinacol ester

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-(4-(trifluoromethyl)phenyl)cyclopropanecarboxamide

: 1346641-89-1
C₂₆H₁₄F₁₀N₂O

Guidance literature:: With water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone; In tert-Amyl alcohol; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja207607s

Reference yield:

: 1346641-14-2
C₉H₁₆O₂

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-(4-(trifluoromethyl)phenyl)cyclopropanecarboxamide

: 1346641-89-1
C₂₆H₁₄F₁₀N₂O

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / 1,4-dioxane / 20 °C

2: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

3: toluene / 12 h / Reflux

4: water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone / tert-Amyl alcohol / 12 h / 100 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone; In 1,4-dioxane; tert-Amyl alcohol; dichloromethane; toluene;
DOI:10.1021/ja207607s

Reference yield:

: 773-82-0
Pentafluorobenzonitrile

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-(4-(trifluoromethyl)phenyl)cyclopropanecarboxamide

: 1346641-89-1
C₂₆H₁₄F₁₀N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / water; ethyl acetate / 6 h / 20 °C

2: toluene / 12 h / Reflux

3: water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone / tert-Amyl alcohol / 12 h / 100 °C / Inert atmosphere

With ammonia; water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone; In tert-Amyl alcohol; water; ethyl acetate; toluene;
DOI:10.1021/ja207607s