methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Base Information

Chemical Name:methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside
CAS No.:115493-90-8
Molecular Formula:C₂₇H₃₄N₆O₇
Molecular Weight:554.603
Hs Code.:

Synonyms:methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

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Chemical Property of methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

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Technology Process of methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

There total 13 articles about methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 115493-89-5
methyl 4-azido-2-O-acetyl-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 115493-90-8
methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: With sodium methylate; for 8h; Ambient temperature;
DOI:10.1016/0008-6215(88)85094-8

Reference yield:

: 115196-83-3
methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 115493-90-8
methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / pyridine

2: 100 percent / H₂SO₄

3: 84 percent / ZnCl₂, dichloromethyl methyl ether / CH₂Cl₂ / 2 h / 35 °C

4: 93 percent / 2,4,6-trimethylpyridine, AgOTf / CH₂Cl₂ / 0.17 h / -25 °C

5: 100 percent / NaOMe

With pyridine; 2,4,6-trimethyl-pyridine; Dichloromethyl methyl ether; sulfuric acid; sodium methylate; silver trifluoromethanesulfonate; zinc(II) chloride; In dichloromethane;

Reference yield:

: 115479-46-4
methyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 115493-90-8
methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl(1→2)4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂SO₄

2: 84 percent / ZnCl₂, dichloromethyl methyl ether / CH₂Cl₂ / 2 h / 35 °C

3: 93 percent / 2,4,6-trimethylpyridine, AgOTf / CH₂Cl₂ / 0.17 h / -25 °C

4: 100 percent / NaOMe

With 2,4,6-trimethyl-pyridine; Dichloromethyl methyl ether; sulfuric acid; sodium methylate; silver trifluoromethanesulfonate; zinc(II) chloride; In dichloromethane;