1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

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Chemical Name:1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol
CAS No.:1004305-70-7
Molecular Formula:C₂₃H₂₀N₂O₃
Molecular Weight:372.423
Hs Code.:

Synonyms:1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

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Chemical Property of 1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

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Technology Process of 1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

There total 3 articles about 1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 893736-16-8
3-(3-benzyloxy-phenyl)-benzaldehyde

: 1004305-70-7
1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

Guidance literature:: 2-methyl-[1,3,4]-oxadiazole; With n-butyllithium; magnesium bromide diethyl etherate; In tetrahydrofuran; hexane; at -78 - -45 ℃; for 2.16667h;

3-(3-benzyloxy-phenyl)-benzaldehyde; In tetrahydrofuran; hexane; at -78 - -45 ℃; for 2h;

Reference yield: 50.0%

: 3451-51-2
2-methyl-[1,3,4]-oxadiazole

: 893736-16-8
3-(3-benzyloxy-phenyl)-benzaldehyde

: 1004305-70-7
1-(3'-benzyloxy-1,1'-biphenyl-3-yl)-1-(5-methyl-1,3 ,4-oxadiazol-2-yl)-methanol

Guidance literature:: 2-methyl-[1,3,4]-oxadiazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

With magnesium bromide ethyl etherate; In tetrahydrofuran; hexane; at -45 ℃; for 2h;

3-(3-benzyloxy-phenyl)-benzaldehyde; With water; ammonium chloride; more than 3 stages;