rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane

Base Information

• Chemical Name: rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane
• CAS No.: 100460-90-0
• Molecular Formula: C₁₇H₁₇Cl₂NO₂
• Molecular Weight: 338.233

Synonyms:rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane

Chemical Property of rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane

There total 1 articles about rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.0^2,9.0^4,7>tridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

(1S,2R,7R,8R)-4-(4-Chloro-phenyl)-3-oxa-5-aza-tricyclo[6.2.1.02,7]undec-4-ene (94098-57-4,112838-20-7) + chloroacetyl chloride (79-04-9) → rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-p-chlorophenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.02,9.04,7>tridecane (100460-90-0)

Guidance literature:

With TEA; In benzene; at 50 ℃; for 0.166667h;

DOI:10.1016/S0040-4020(01)96486-5

upstream raw materials:

(1S,2R,7R,8R)-4-(4-Chloro-phenyl)-3-oxa-5-aza-tricyclo[6.2.1.0^2,7]undec-4-ene

chloroacetyl chloride

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