α,β-dideuteriobenzhydrol

Base Information

• Chemical Name: α,β-dideuteriobenzhydrol
• CAS No.: 74563-00-1
• Molecular Formula: C₁₃H₁₂O
• Molecular Weight: 186.222
• Mol file: 74563-00-1.mol

Synonyms:α,β-dideuteriobenzhydrol

Chemical Property of α,β-dideuteriobenzhydrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,β-dideuteriobenzhydrol

There total 5 articles about α,β-dideuteriobenzhydrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzophenone (119-61-9) → α,β-dideuteriobenzhydrol (74563-00-1)

Guidance literature:

benzophenone; With lithium vanadium(I) dihydride; In tetrahydrofuran; at 25 ℃; for 12h; Inert atmosphere;

With water-d2;

DOI:10.1002/ejoc.200800461

Reference yield:

benzophenone (119-61-9) → 1,1-Diphenylmethanol (91-01-0) + α,β-dideuteriobenzhydrol (74563-00-1)

Guidance literature:

benzophenone; In tetrahydrofuran; at 20 ℃;

With water-d2; In tetrahydrofuran; Further stages.;

DOI:10.1016/j.jorganchem.2007.06.045

Reference yield:

benzophenone (119-61-9) → α,β-dideuteriobenzhydrol (74563-00-1) + benzhydrol-O-d (90718-39-1)

Guidance literature:

With hydrogen; (-)-sparteine; [(COD)Ir{(1R,2S)-Ph₂PCH(Ph)(CH)(Me)NHMe}]BF₄; In deuteromethanol; at 50 ℃; for 10h; under 7500.6 Torr; Further Variations:; Catalysts; Product distribution;

DOI:10.1002/ejic.200300503

upstream raw materials:

benzophenone

diphenylcarbene