(E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

Base Information

Chemical Name:(E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate
CAS No.:1092400-39-9
Molecular Formula:C₂₀H₂₄O₇
Molecular Weight:376.406
Hs Code.:

Synonyms:(E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

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Chemical Property of (E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

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Technology Process of (E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

There total 2 articles about (E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 107473-14-3
dimethyl 2-propargyl-2-prenylmalonate

: 1092400-39-9
(E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

: dimethyl 1,1-dimethyl-3-(3,4,5-trimethoxyphenyl)-3,5,7,7a-tetrahydrocyclopenta[c]pyran-6,6(1H)-dicarboxylate

: 67-64-1
acetone

Guidance literature:: 3,4,5-trimethoxy-benzaldehyde; dimethyl 2-propargyl-2-prenylmalonate; In dichloromethane; at -40 ℃; for 0.25h; Inert atmosphere;

With C₄₉H₆₈AuNP⁽¹⁺⁾*F₆Sb^(1-); In dichloromethane; at -40 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.200900668

Reference yield:

: 1092400-30-0
(E)-dimethyl 2-(prop-2-ynyl)-2-(3-(3,4,5-trimethoxyphenyl)allyl)malonate

: C₂₀H₂₄O₇

: 1092400-38-8
(Z)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

: 1092400-39-9
(E)-dimethyl 3-(3,4,5-trimethoxystyryl)cyclopent-3-ene-1,1-dicarboxylate

Guidance literature:: With platinum(IV) chloride; In dichloromethane; at 20 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1002/anie.200803269