C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃

Base Information

• Chemical Name: C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃
• CAS No.: 122171-43-1
• Molecular Formula: CF₃O₃S*C₁₇H₁₉FeO₂S
• Molecular Weight: 492.32
• Mol file: 122171-43-1.mol

Synonyms:C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃

Chemical Property of C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃

There total 1 articles about C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=C₅H₅(CO)2Fe(CH₂)3S(CH₃)C₆H₅CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

C5H5(CO)2Fe(CH2)3SC6H5 (122171-44-2) + methyl trifluoromethanesulfonate (333-27-7) → C5H5(CO)2Fe(CH2)3S(CH3)C6H5(1+)*CF3SO3(1-)=C5H5(CO)2Fe(CH2)3S(CH3)C6H5CF3SO3 (122171-43-1)

Guidance literature:

In dichloromethane; stirring in the dark at room temp. for 12h (inert atmosphere); evapn. under high vac. (thick red oil); washing (hexane); drying in vac.;

DOI:10.1021/om00038a036

Reference yield:

C5H5(CO)2Fe(CH2)3S(CH3)C6H5(1+)*CF3SO3(1-)=C5H5(CO)2Fe(CH2)3S(CH3)C6H5CF3SO3 (122171-43-1) → cyclopropane (75-19-4)

Guidance literature:

In dichloromethane; heating to 65 °C;

DOI:10.1021/om00111a038

upstream raw materials:

C₅H₅(CO)2Fe(CH₂)3SC₆H₅

methyl trifluoromethanesulfonate

Downstream raw materials:

cyclopropane