Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

Base Information

Chemical Name:Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside
CAS No.:139760-21-7
Molecular Formula:C₃₁H₃₇NO₇
Molecular Weight:535.637
Hs Code.:

Synonyms:Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

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Chemical Property of Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

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Technology Process of Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

There total 4 articles about Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.2%

: 100-39-0
benzyl bromide

: 139760-20-6
Methyl 2-acetamido-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

: 139760-21-7
Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; for 4h; Ambient temperature;
DOI:10.1021/jo00034a047

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 139760-21-7
Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / KOH / dimethylsulfoxide / 1 h / Ambient temperature

2: 85.5 percent / 1percent methanolic iodine / 6 h / Heating

3: 79.2 percent / KOH / dimethylsulfoxide / 4 h / Ambient temperature

With potassium hydroxide; iodine; In dimethyl sulfoxide;
DOI:10.1021/jo00034a047

Reference yield:

: 6748-94-3
methyl 2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 139760-21-7
Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: wet Amberlite IRA 400 (OH^--form) / methanol / 4 h / 40 °C

2: 88 percent / KOH / dimethylsulfoxide / 1 h / Ambient temperature

3: 85.5 percent / 1percent methanolic iodine / 6 h / Heating

4: 79.2 percent / KOH / dimethylsulfoxide / 4 h / Ambient temperature

With potassium hydroxide; Amberlite IRA 400 (OH^--form); iodine; In methanol; dimethyl sulfoxide;
DOI:10.1021/jo00034a047