5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

Base Information

Chemical Name:5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one
CAS No.:1500092-70-5
Molecular Formula:C₁₇H₁₃ClN₂O₆S
Molecular Weight:408.819
Hs Code.:

Synonyms:5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

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Chemical Property of 5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

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Technology Process of 5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

There total 3 articles about 5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₀ClNO₂

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1500092-70-5
5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

Guidance literature:: C₁₁H₁₀ClNO₂; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.25h; Inert atmosphere;

4-Nitrobenzenesulfonyl chloride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jacs.0c00078

Reference yield:

: 5467-71-0
4-chlorophenacylamine hydrochloride

: 1500092-70-5
5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / methanol; water

2.1: 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.0c00078

Reference yield:

: 778617-69-9
2-[N-(tert-butoxycarbonyl)amino]-1-(4-chlorophenyl)ethanone

: 1500092-70-5
5-(4-chlorophenyl)-3-((4-nitrophenyl)sulfonyl)-5-vinyloxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jacs.0c00078