5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Base Information

Chemical Name:5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate
CAS No.:98290-99-4
Molecular Formula:C₃₅H₃₉N₅O₆
Molecular Weight:625.725
Hs Code.:

Synonyms:5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

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Chemical Property of 5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

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Technology Process of 5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

There total 4 articles about 5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.5%

: 65867-28-9
3,3-diamino-acrylic acid ethyl ester hydrochloride

: 90120-00-6
2-(4-diphenylmethyl-1-piperazinyl)ethyl 2-(3-nitrobenzylidene)acetoacetate

: 98290-99-4
5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: With sodium; In ethanol; for 0.0833333h; Heating;
DOI:10.1248/cpb.33.3787

Reference yield:

ethyl ether-ethyl acetate: ethyl ether-ethyl acetate

: 2-(4-benzhydryl-1-piperazinyl)ethyl 2-(3-nitrobenzylidene)acetoacetate

: 57508-48-2
carbethoxyacetamidine hydrochloride

: 98290-99-4
5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: With sodium ethanolate; sodium; In ethanol;

Reference yield:

: 10527-64-7
1-diphenylmethyl-4-(2-hydroxyethyl)piperazine

: 98290-99-4
5-<2-(4-diphenylmethyl-1-piperazinyl)ethyl> 3-ethyl 2-amino-1,4-dihydro-6-methyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 739.8 g / 2 h / 70 - 80 °C

2: piperidine / benzene / 5 h / Heating

3: 60.5 percent / Na / ethanol / 0.08 h / Heating

With piperidine; sodium; In ethanol; benzene;
DOI:10.1248/cpb.33.3787