(3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester

Base Information

• Chemical Name: (3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester
• CAS No.: 945650-70-4
• Molecular Formula: C₃₅H₃₇N₃O₇
• Molecular Weight: 611.695

Synonyms:(3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester

Chemical Property of (3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester

There total 1 articles about (3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

BOC-L-aspartic acid 4-benzyl ester (7536-58-5,98482-77-0) + (3S)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester (102130-85-8) → (3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester (945650-70-4)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 1h;

DOI:10.1016/j.bmc.2007.06.012

Reference yield:

(3S)-N-[Boc-L-aspartyl(OBzl)]-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester (945650-70-4) → (3S,12aS)-3-(benzyloxycarbonylmethyl)-2,3,6,7,12,12a-hexahydropyrazino[1',2':1,6]pyrido[3,4-b]indole-1,4-dione (944073-28-3)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2007.06.012

upstream raw materials:

BOC-L-aspartic acid 4-benzyl ester

(3S)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid benzyl ester

Downstream raw materials:

(3S,12aS)-3-(benzyloxycarbonylmethyl)-2,3,6,7,12,12a-hexahydropyrazino[1',2':1,6]pyrido[3,4-b]indole-1,4-dione

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