tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

Base Information

Chemical Name:tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate
CAS No.:1192544-75-4
Molecular Formula:C₁₆H₂₃NO₅S
Molecular Weight:341.428
Hs Code.:

Synonyms:tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

Suppliers and Price of tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

There total 1 articles about tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1192544-74-3
tert-butyl (2S)-N-(3-hydroxy-2-methylpropyl)-N-(toluene-4-sulfonyl)carbamate

: 1192544-75-4
tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1016/j.tet.2009.07.060

Reference yield: 68.0%

: 1192544-75-4
tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

: 56069-39-7
diethyl phenylsulfonylmethylphosphonate

: 1192544-78-7
tert-butyl (2R,3E)-N-(2-methyl-4-(phenylsulfonyl)but-3-enyl)-N-(toluene-4-sulfonyl)carbamate

Guidance literature:: diethyl phenylsulfonylmethylphosphonate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2009.07.060

Reference yield: 56.0%

: 1192544-75-4
tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate

: 1779-49-3
Methyltriphenylphosphonium bromide

: tert-butyl (2R)-N-(2-methylbut-3-enyl)-N-(toluene-4-sulfonyl)carbamate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 1h; Inert atmosphere;

tert-butyl (2S)-N-(2-methyl-3-oxopropyl)-N-(toluene-4-sulfonyl)carbamate; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.060