(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

Base Information

Chemical Name:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol
CAS No.:1005519-97-0
Molecular Formula:C₃₆H₇₂S₂Si₇
Molecular Weight:765.698
Hs Code.:

Synonyms:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

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Chemical Property of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

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Technology Process of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

There total 4 articles about (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 135865-41-7
1,2,3,4,5-tetrathiasilolane

: 1005519-97-0
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/ejic.200601226

Reference yield: 41.0%

: (Z)-1,2-dimesityl-1,2-bis{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}disilene

: 1005519-97-0
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

: 135865-41-7
1,2,3,4,5-tetrathiasilolane

Guidance literature:: (Z)-1,2-dimesityl-1,2-bis{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}disilene; In tetrahydrofuran; at 60 ℃; for 20h;

With water; In tetrahydrofuran; benzene; Further stages.;
DOI:10.1002/ejic.200601226

Reference yield: 41.0%

: 185910-18-3
1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene

: 1005519-97-0
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-(2,4,6-trimethylphenyl)silanedithiol

: 135865-41-7
1,2,3,4,5-tetrathiasilolane

Guidance literature:: 1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene; With zirconocene pentasulfide; In tetrahydrofuran; at 60 ℃; for 20h; Inert atmosphere;

In benzene;
DOI:10.1016/j.jorganchem.2008.11.001