methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside
CAS No.:129172-14-1
Molecular Formula:C₁₉H₂₅NO₈
Molecular Weight:395.409
Hs Code.:

Synonyms:methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

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Technology Process of methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

There total 4 articles about methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 29617-66-1
(S)-2-chloropropanoic acid

: 87038-18-4
methyl 2-acetylamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 129172-14-1
methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jo035397e

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 129172-14-1
methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / BF₃*Et₂O / methanol / 20 °C

2: NaOMe / methanol / 0.5 h / 20 °C

3: p-toluenesulfonic acid monohydrate / acetonitrile / 2 h / 20 °C

4: 59 percent / molecular sieves 4 Angstroem; NaH / dimethylformamide / 20 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo035397e

Reference yield:

: 3946-01-8
methyl N-acetyl-β-D-glucosaminide

: 129172-14-1
methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / acetonitrile / 2 h / 20 °C

2: 59 percent / molecular sieves 4 Angstroem; NaH / dimethylformamide / 20 °C

With 4 A molecular sieve; sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo035397e