methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Base Information

Chemical Name:methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt
CAS No.:1266211-65-7
Molecular Formula:C₂₁H₂₈NO₉*Na
Molecular Weight:461.444
Hs Code.:

Synonyms:

Suppliers and Price of methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

There total 6 articles about methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129172-14-1
methyl 2-acetamido-4,6-O-benzylidene-3-O-((R)-1'-carboxyethyl)-2-deoxy-β-D-glucopyranoside

: 1266211-65-7
methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; diethyl ether; toluene / 1.5 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 1.5 h / -78 °C / Inert atmosphere; Molecular sieve

2.1: triethylsilane / dichloromethane / -78 °C / Molecular sieve; Inert atmosphere

2.2: -78 °C / Molecular sieve; Inert atmosphere

3.1: lithium hydroxide / 1,4-dioxane; methanol / 20 °C / pH 10

4.1: pyridine / 0 - 20 °C / Inert atmosphere

5.1: dichloromethane

6.1: Amberlite IR-120(Na⁺) / water

With pyridine; triethylsilane; lithium hydroxide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1021/jo102329c

Reference yield:

: 1266211-77-1
methyl 2-acetamido-4-O-benzyl-2-deoxy-3-O-((R)-1-(methoxycarbonyl)ethyl)-β-D-glucopyranoside

: 1266211-65-7
methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hydroxide / 1,4-dioxane; methanol / 20 °C / pH 10

2: pyridine / 0 - 20 °C / Inert atmosphere

3: dichloromethane

4: Amberlite IR-120(Na⁺) / water

With pyridine; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1021/jo102329c

Reference yield:

: C₁₉H₂₇NO₈

: 1266211-65-7
methyl 2-acetamido-6-O-acetyl-4-O-benzyl-3-O-((R)-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside monosodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: dichloromethane

3: Amberlite IR-120(Na⁺) / water

With pyridine; In dichloromethane; water;
DOI:10.1021/jo102329c