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methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate

Base Information Edit
  • Chemical Name:methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate
  • CAS No.:729614-30-6
  • Molecular Formula:C22H23NO2
  • Molecular Weight:333.43
  • Hs Code.:
  • Mol file:729614-30-6.mol
methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate

Synonyms:methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate

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Chemical Property of methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate Edit
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Technology Process of methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate

There total 6 articles about methyl 5-benzyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
methyl 5,6,7,8,9,10-hexahydrocyclohepta[b]indole-4-carboxylate; With potassium hydroxide; In dimethyl sulfoxide; for 0.0833333h;
benzyl bromide; In dimethyl sulfoxide; for 0.166667h;
Guidance literature:
With norborn-2-ene; caesium carbonate; palladium(II) bromide; tris(para-trifluoromethyl)phenyl phosphine; In para-xylene; acetonitrile; at 130 ℃; for 14h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0040-1720693
Guidance literature:
Multi-step reaction with 2 steps
1: zinc / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere; Schlenk technique
2: palladium(II) bromide; caesium carbonate; norborn-2-ene; tris(para-trifluoromethyl)phenyl phosphine / acetonitrile; para-xylene / 14 h / 130 °C / Inert atmosphere; Schlenk technique
With norborn-2-ene; caesium carbonate; palladium(II) bromide; zinc; tris(para-trifluoromethyl)phenyl phosphine; In para-xylene; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0040-1720693
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