methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

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Chemical Name:methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate
CAS No.:1234693-25-4
Molecular Formula:C₂₁H₂₁NO₄
Molecular Weight:351.402
Hs Code.:

Synonyms:methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

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Technology Process of methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

There total 2 articles about methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 913344-41-9
2-((S)-1-Phenyl-allyl)-isoindole-1,3-dione

: 201230-82-2
carbon monoxide

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 1234693-15-2
methyl (2E,6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhex-2-enoate

: 1234693-25-4
methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

Guidance literature:: With (acetylacetonato)dicarbonylrhodium (l); hydrogen; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin); In toluene; at 50 ℃; for 5h; under 750.075 Torr; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000016

Reference yield:

: 913344-41-9
2-((S)-1-Phenyl-allyl)-isoindole-1,3-dione

: 201230-82-2
carbon monoxide

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 1234693-25-4
methyl (6S)-6-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-6-phenylhexanoate

Guidance literature:: 2-((S)-1-Phenyl-allyl)-isoindole-1,3-dione; carbon monoxide; methyl (triphenylphosphoranylidene)acetate; With (acetylacetonato)dicarbonylrhodium (l); hydrogen; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin); In toluene; at 50 ℃; for 5h; under 750.075 Torr; Inert atmosphere;

With Pd(OH)2/C; hydrogen; In ethyl acetate; at 20 ℃; for 1h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/adsc.201000016