7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

Base Information

Chemical Name:7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid
CAS No.:1398695-49-2
Molecular Formula:CH₄O₃S*C₂₄H₂₆N₂O₂
Molecular Weight:470.59
Hs Code.:

Synonyms:7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

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Chemical Property of 7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

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Technology Process of 7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

There total 2 articles about 7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-75-2,98527-29-8
methanesulfonic acid

: 1398695-47-0
7-(2-(methyloxy)-6-{[(4-methyl-2-pyridinyl)methyl]oxy}phenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

: 1398695-49-2
7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

Guidance literature:: In isopropyl alcohol; at 40 ℃; for 1h;

Reference yield:

: 1398697-34-1
tert-butyl 7-(2-methoxy-6-((4-methylpyridin-2-yl)methoxy)phenyl)-4,5-dihydro-1H-benzo[d]azepine-3(2H)-carboxylate

: 1398695-49-2
7-{2-methoxy-6-[(4-methylpyridin-2-yl)methoxy]phenyl}-2,3,4,5-tetrahydro-1H-3-benzazepine methanesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 1.5 h

2: isopropyl alcohol / 1 h / 40 °C

With hydrogenchloride; In 1,4-dioxane; isopropyl alcohol;