toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester
CAS No.:1431372-78-9
Molecular Formula:C₁₁H₁₄O₃S
Molecular Weight:228.28
Hs Code.:

Synonyms:toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

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Technology Process of toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

There total 1 articles about toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71010-13-4
2-methylprop-2-en-1,1-d₂-1-ol

: 98-59-9
p-toluenesulfonyl chloride

: 1431372-78-9
toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

Guidance literature:: With trimethylamine hydrochloride; triethylamine; In toluene; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol400574s

Reference yield: 93.0%

: 1431372-78-9
toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 1431372-77-8
[(E)-3-(1,1-dideuterio-2-methylallyloxy)prop-1-enyl]benzene

Guidance literature:: (2E)-3-phenyl-2-propen-1-ol; With sodium hydride; In 1-methyl-pyrrolidin-2-one; paraffin oil; at 0 ℃; for 0.5h; Inert atmosphere;

toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester; In 1-methyl-pyrrolidin-2-one; paraffin oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol400574s

Reference yield: 65.0%

: 1431372-78-9
toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester

: 346621-58-7
dimethyl 2-(3-phenylprop-2-yn-1-yl)malonate

: 1609650-46-5
2-(1,1-dideuterated-2-methylallyl)-2-(3-phenylprop-2-ynyl)malonic acid dimethyl ester

Guidance literature:: dimethyl 2-(3-phenylprop-2-yn-1-yl)malonate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

toluene-4-sulfonic acid 1,1-dideuterated-2-methylallyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja504048u