methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

Base Information

Chemical Name:methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester
CAS No.:1616924-29-8
Molecular Formula:C₁₄H₁₇F₃O₃S
Molecular Weight:322.348
Hs Code.:

Synonyms:methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

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Chemical Property of methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

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Technology Process of methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

There total 4 articles about methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.6%

: 1616924-28-7
[1-(4-trifluoromethylphenyl)cyclopentyl]methanol

: 124-63-0
methanesulfonyl chloride

: 1616924-29-8
methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield:

: 2338-75-2
4-(Trifluoromethyl)phenylacetonitrile

: 1616924-29-8
methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / diethyl ether; dimethyl sulfoxide / 2 h / 0 °C

2: diisobutylaluminium hydride / toluene; dichloromethane / 2 h / -70 °C

3: sodium tetrahydroborate; methanol / 2 h / 0 - 20 °C

4: triethylamine / dichloromethane / 1 h / 0 - 20 °C

With methanol; sodium tetrahydroborate; sodium hydride; diisobutylaluminium hydride; triethylamine; In diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 483368-74-7
1-(4-(trifluoromethyl)phenyl)cyclopentane-1-carbaldehyde

: 1616924-29-8
methanesulfonic acid 1-(4-trifluoromethylphenyl)cyclopentylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 2 h / 0 - 20 °C

2: triethylamine / dichloromethane / 1 h / 0 - 20 °C

With methanol; sodium tetrahydroborate; triethylamine; In dichloromethane;