phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:1083236-91-2
Molecular Formula:C₃₁H₃₄O₇S
Molecular Weight:550.673
Hs Code.:

Synonyms:phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 158716-08-6
phenyl 4,6-O-benzylidene-2-O-benzyl-1-deoxy-1-thio-α-D-mannopyranoside

: 1083236-91-2
phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo801630m

Reference yield: 90.0%

: 1083236-91-2
phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 1083236-92-3
phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside S-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - -30 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1021/jo801630m

Reference yield: 69.0%

: 1083236-91-2
phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 108-93-0
cyclohexanol

: 1083236-93-4
cyclohexyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Guidance literature:: phenyl 3-O-tert-butoxycarbonyl-2-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside; With 1-(phenylsulfonyl)piperidine; 2,4,5-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;

With trifluoromethylsulfonic anhydride; In dichloromethane; Inert atmosphere; Cooling;

cyclohexanol; In dichloromethane; at -60 ℃; for 2h;
DOI:10.1021/jo801630m