1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

Base Information

Chemical Name:1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate
CAS No.:1229246-26-7
Molecular Formula:C₂₀H₃₁NO₃
Molecular Weight:333.471
Hs Code.:

Synonyms:1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

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Chemical Property of 1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

There total 6 articles about 1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229246-27-8
1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

: 1229246-26-7
1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 2h;

Reference yield:

: 1229246-30-3
N-[(5-chloro-2-methylphenyl)methyl]cyclopropanamine

: 1229246-26-7
1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C

1.2: 2 h / -78 - 20 °C

2.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / butan-1-ol / 16 h / 100 °C / Inert atmosphere of nitrogen

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; hydrogen; potassium hexamethylsilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium 10% on activated carbon; In tetrahydrofuran; ethyl acetate; toluene; butan-1-ol; 2.1: Suzuki Coupling;

Reference yield:

: 1229246-31-4
5-chloro-N-cyclopropyl-2-methylbenzamide

: 1229246-26-7
1,1-dimethylethyl cyclopropyl({2-methyl-5-[3-(methyloxy)propyl]phenyl}methyl)-carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: borane / tetrahydrofuran / 2 h / 0 °C / Heating; Reflux

1.2: 0 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C

2.2: 2 h / -78 - 20 °C

3.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / butan-1-ol / 16 h / 100 °C / Inert atmosphere of nitrogen

4.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; borane; hydrogen; potassium hexamethylsilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium 10% on activated carbon; In tetrahydrofuran; ethyl acetate; toluene; butan-1-ol; 3.1: Suzuki Coupling;