1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

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Chemical Name:1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate
CAS No.:1229246-27-8
Molecular Formula:C₂₀H₂₉NO₃
Molecular Weight:331.455
Hs Code.:

Synonyms:1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

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Chemical Property of 1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

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Technology Process of 1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

There total 5 articles about 1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229246-29-0
1,1-dimethylethyl [(5-chloro-2-methylphenyl)methyl]cyclopropylcarbamate

: 165059-42-7,934342-48-0
(E)-3-methoxy-1-propenylboronic acid pinacol ester

: 1229246-27-8
1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In butan-1-ol; at 100 ℃; for 16h; Inert atmosphere of nitrogen;

Reference yield:

: 1229246-30-3
N-[(5-chloro-2-methylphenyl)methyl]cyclopropanamine

: 1229246-27-8
1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C

1.2: 2 h / -78 - 20 °C

2.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / butan-1-ol / 16 h / 100 °C / Inert atmosphere of nitrogen

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; potassium hexamethylsilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; toluene; butan-1-ol; 2.1: Suzuki Coupling;

Reference yield:

: 1229246-31-4
5-chloro-N-cyclopropyl-2-methylbenzamide

: 1229246-27-8
1,1-dimethylethyl cyclopropyl({2-methyl-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: borane / tetrahydrofuran / 2 h / 0 °C / Heating; Reflux

1.2: 0 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C

2.2: 2 h / -78 - 20 °C

3.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / butan-1-ol / 16 h / 100 °C / Inert atmosphere of nitrogen

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; borane; potassium hexamethylsilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; toluene; butan-1-ol; 3.1: Suzuki Coupling;