(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

Base Information

Chemical Name:(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol
CAS No.:1534390-93-6
Molecular Formula:C₃₄H₃₉NO₄
Molecular Weight:525.688
Hs Code.:

Synonyms:(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

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Chemical Property of (2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

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Technology Process of (2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

There total 9 articles about (2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1534390-95-8
(R)-1-((R)-1-phenylethyl)-2-((1S,2S)-1,2,3-tris(benzyloxy)propyl)aziridine

: 1534390-93-6
(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

Guidance literature:: (R)-1-((R)-1-phenylethyl)-2-((1S,2S)-1,2,3-tris(benzyloxy)propyl)aziridine; With acetic acid; In dichloromethane; at 20 ℃; for 18h;

With potassium hydroxide; In ethanol; at 20 ℃; for 2h;

Reference yield:

: C₃₆H₄₁NO₅

: 1534390-93-6
(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

Guidance literature:: With ethanol; potassium hydroxide; at 20 ℃; for 2h;
DOI:10.1055/s-0033-1338545

Reference yield:

: ethyl 2,3-dihydroxy-3-{(R)-1-[(R)-1-phenylethyl]aziridin-2-yl}propanoate

: 1534390-93-6
(2R,3S,4S)-3,4,5-tris(benzyloxy)-2-(((R)-1-phenylethyl)amino)pentan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

2.2: 12 h / 20 °C

3.1: dichloromethane / 18 h / 20 °C

4.1: potassium hydroxide; ethanol / 2 h / 20 °C

With lithium aluminium tetrahydride; ethanol; sodium hydride; potassium hydroxide; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1055/s-0033-1338545