2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl)

Base Information

• Chemical Name: 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl)
• CAS No.: 391689-21-7
• Molecular Formula: C₅₅H₁₀₂BNSi₇
• Molecular Weight: 984.831

Synonyms:2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl)

Chemical Property of 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl)

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Technology Process of 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl)

There total 3 articles about 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH₂BH(mesityl)CN(2,4,6-tri-tert-butylphenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiHBH2CN(2,4,6-tri-tert-butylphenyl) → 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH2BH(mesityl)CN(2,4,6-tri-tert-butylphenyl) (391689-21-7)

Guidance literature:

In benzene-d6; High Pressure; (Ar); heating a soln. of boron compd. in C6D6 at 120°C in the dark in a sealed NMR tube for 18 h, cooling to room temp.; PTLC (SiO2, hexane); elem. anal.;

DOI:10.1021/om049558w

Reference yield:

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiHBH2PPh3 (781640-92-4) + 2,4,6‐tri‐tert‐butylphenylisocyanide (69847-28-5) → 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH2BH(mesityl)PPh3 + 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH2BH(mesityl)CN(2,4,6-tri-tert-butylphenyl) (391689-21-7) + 2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiHBH2CN(2,4,6-tri-tert-butylphenyl)

Guidance literature:

In benzene-d6; (Ar); heating a soln. of boron compd. and isonitrile in C6D6 at 80°C in a sealed NMR tube for 4 h, cooling to room temp.; detected by NMR;

DOI:10.1021/om049558w

Reference yield:

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiCN(2,4,6-tri-tert-butylphenyl) → 2,4,6-tris[bis(trimethylsilyl)methyl]phenylSiH2BH(mesityl)CN(2,4,6-tri-tert-butylphenyl) (391689-21-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: benzene-d6

In tetrahydrofuran; benzene-d6;

DOI:10.1246/cl.2001.1076

upstream raw materials:

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiHBH₂PPh₃

2,4,6‐tri‐tert‐butylphenylisocyanide

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