N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

Base Information

Chemical Name:N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide
CAS No.:1529768-96-4
Molecular Formula:C₁₆H₁₆FN₃O₂
Molecular Weight:301.32
Hs Code.:

Synonyms:N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

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Chemical Property of N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

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Technology Process of N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

There total 4 articles about N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1529768-94-2
N-[4-(2-fluoro-4-nitro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

: 1529768-96-4
N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 6914-76-7
1-Methyl-cyclopropanoic acid

: 1529768-96-4
N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 0 - 20 °C

2: triethylamine / dichloromethane / 15 h / 0 - 20 °C

3: palladium 10% on activated carbon; hydrogen / dichloromethane / 2 h / 20 °C

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; triethylamine; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 16480-05-0
1-methylcyclopropanecarbonyl chloride

: 1529768-96-4
N-[4-(4-amino-2-fluoro-phenoxy)-2-pyridyl]-1-methyl-cyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 15 h / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / dichloromethane / 2 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In dichloromethane;