C₂₉H₂₈FNO₇S

Base Information

Chemical Name:C₂₉H₂₈FNO₇S
CAS No.:1374234-43-1
Molecular Formula:C₂₉H₂₈FNO₇S
Molecular Weight:553.608
Hs Code.:

C<sub>29</sub>H<sub>28</sub>FNO<sub>7</sub>S

Synonyms:C₂₉H₂₈FNO₇S

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Chemical Property of C₂₉H₂₈FNO₇S

Chemical Property:

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Technology Process of C₂₉H₂₈FNO₇S

There total 9 articles about C₂₉H₂₈FNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374234-42-0
C₃₂H₃₄FNO₇S

: 1374234-43-1
C₂₉H₂₈FNO₇S

Guidance literature:: C₃₂H₃₄FNO₇S; With boron trichloride; In dichloromethane; at -30 ℃; for 2h; Inert atmosphere;

With water; In dichloromethane; Cooling with ice;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-43-1
C₂₉H₂₈FNO₇S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

7.1: pyridine / dichloromethane / 3 h / 0 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

9.1: boron trichloride / dichloromethane / 2 h / -30 °C / Inert atmosphere

9.2: Cooling with ice

With pyridine; potassium phosphate; hydrogen; nitric acid; boron trichloride; sodium hydride; potassium carbonate; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-43-1
C₂₉H₂₈FNO₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

6.1: pyridine / dichloromethane / 3 h / 0 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

8.1: boron trichloride / dichloromethane / 2 h / -30 °C / Inert atmosphere

8.2: Cooling with ice

With pyridine; potassium phosphate; hydrogen; nitric acid; boron trichloride; potassium carbonate; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;