10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

Base Information

Chemical Name:10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene
CAS No.:116511-39-8
Molecular Formula:C₂₆H₃₄O₃Si
Molecular Weight:422.64
Hs Code.:

Synonyms:10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

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Chemical Property of 10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

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Technology Process of 10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

There total 3 articles about 10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 116511-38-7
5-<(tert-butyldiphenylsilyloxy)methyl>-4-methoxy-1-methyl-1,3-cyclohexadiene

: 107-21-1
ethylene glycol

: 116511-39-8
10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 16h; Heating; Dean-Stark conditions;
DOI:10.1016/S0040-4020(01)89182-1

Reference yield:

: 127785-50-6
5-hydroxymethyl-4-methoxy-1-methyl-1,3-cyclohexadiene

: 116511-39-8
10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 18 h / 0 °C

2: 88 percent / pyridinium-p-toluenesulphonate / benzene / 16 h / Heating; Dean-Stark conditions

With dmap; pyridinium p-toluenesulfonate; triethylamine; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)89182-1

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 116511-39-8
10-<(tert-butyldiphenylsilyloxy)methyl>-8-methyl-1,4-dioxaspiro<4.5>dec-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 18 h / 0 °C

2: 88 percent / pyridinium-p-toluenesulphonate / benzene / 16 h / Heating; Dean-Stark conditions

With dmap; pyridinium p-toluenesulfonate; triethylamine; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)89182-1