6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

Base Information

Chemical Name:6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide
CAS No.:1620101-26-9
Molecular Formula:C₂₁H₂₂N₂O₆S
Molecular Weight:430.481
Hs Code.:

Synonyms:6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

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Chemical Property of 6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

Chemical Property:

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Technology Process of 6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

There total 4 articles about 6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941-55-9
4-toluenesulfonyl azide

: 1620101-25-8
6-(2-ethoxy-2-oxoethoxy)-2-methylquinoline N-oxide

: 1620101-26-9
6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; acetic acid; silver(I) triflimide; In 1,2-dichloro-ethane; at 50 ℃; for 5h;
DOI:10.1021/ja5053768

Reference yield:

: 1620101-24-7
ethyl 2-((2-methylquinolin-6-yl)oxy)acetate

: 1620101-26-9
6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h / 50 °C

2: silver(I) triflimide; acetic acid; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / 1,2-dichloro-ethane / 5 h / 50 °C

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; acetic acid; 3-chloro-benzenecarboperoxoic acid; silver(I) triflimide; In chloroform; 1,2-dichloro-ethane;
DOI:10.1021/ja5053768

Reference yield:

: 613-21-8
6-hydroxyquinaldine

: 1620101-26-9
6-(2-ethoxy-2-oxoethoxy)-2-methyl-8-(4-methylphenylsulfonamido)quinoline N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h / 50 °C

3: silver(I) triflimide; acetic acid; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / 1,2-dichloro-ethane / 5 h / 50 °C

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; silver(I) triflimide; In chloroform; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja5053768