4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

Base Information

Chemical Name:4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde
CAS No.:1433748-01-6
Molecular Formula:C₅₀H₄₇N₃O₅
Molecular Weight:769.94
Hs Code.:

Synonyms:4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

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Chemical Property of 4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

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Technology Process of 4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

There total 3 articles about 4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1284287-90-6
2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole

: 1433747-94-4
4,4'-((4'-hydroxy[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

: 1433748-01-6
4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

Guidance literature:: With caesium carbonate; In tetrahydrofuran; at 65 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2013.03.092

Reference yield:

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1433748-01-6
4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 24 h / Inert atmosphere; Reflux

2: caesium carbonate / tetrahydrofuran / 24 h / 65 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; In tetrahydrofuran; water; 2: |Williamson Ether Synthesis;
DOI:10.1016/j.tet.2013.03.092

Reference yield:

: 106-41-2
4-bromo-phenol

: 1433748-01-6
4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 24 h / 80 °C / Inert atmosphere

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 24 h / Inert atmosphere; Reflux

3: caesium carbonate / tetrahydrofuran / 24 h / 65 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; caesium carbonate; In tetrahydrofuran; water; dimethyl sulfoxide; 3: |Williamson Ether Synthesis;
DOI:10.1016/j.tet.2013.03.092