2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole

Base Information

• Chemical Name: 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole
• CAS No.: 1284287-90-6
• Molecular Formula: C₂₄H₂₉BrN₂O₂
• Molecular Weight: 457.41

Synonyms:2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole

Chemical Property of 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole

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Technology Process of 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole

There total 1 articles about 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.6%

1 ,6-dibromohexane (629-03-8) + 2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (292869-69-3) → 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole (1284287-90-6)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 70 ℃; for 24h; Inert atmosphere;

DOI:10.1002/pola.25017

Reference yield: 85.0%

methyl 3-hydroxypicolinate (62733-99-7) + 2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole (1284287-90-6) → methyl 3-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyloxy)picolinate

Guidance literature:

With caesium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1039/d0dt01415j

Reference yield: 83.0%

2-(4-(6-bromohexyloxy)phenyl)-5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazole (1284287-90-6) + 4,4'-((4'-hydroxy[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde (1433747-94-4) → 4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde (1433748-01-6)

Guidance literature:

With caesium carbonate; In tetrahydrofuran; at 65 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2013.03.092

upstream raw materials:

1 ,6-dibromohexane

2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole

Downstream raw materials:

C₄₃H₄₄BrN₃O₃

C₆₁H₆₄Br₂N₄O₄

4,4'-((4'-((6-(4-(5-(4-(tert-butyl)phenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)oxy)[1,1'-biphenyl]-4-yl)azanediyl)dibenzaldehyde

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