5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene

Base Information

Chemical Name:5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene
CAS No.:1035222-36-6
Molecular Formula:C₃₃H₂₈O₄
Molecular Weight:488.583
Hs Code.:

Synonyms:5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene

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Chemical Property of 5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene

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Technology Process of 5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene

There total 1 articles about 5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 111979-80-7
5,6,5',6'-tetramethoxy-1,1'-spirobisindane-3,3'-dione

: 100-58-3
phenylmagnesium bromide

: 1035222-36-6
5,6,5',6'-tetramethoxy-3,3'-diphenyl-1,1'-spirobisindene

Guidance literature:: 5,6,5',6'-tetramethoxy-1,1'-spirobisindane-3,3'-dione; phenylmagnesium bromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With sulfuric acid; In water; at 90 ℃; for 20h;
DOI:10.1021/ol800573m