4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

Base Information

Chemical Name:4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide
CAS No.:1104636-95-4
Molecular Formula:C₁₇H₂₃B₂NO₆
Molecular Weight:358.995
Hs Code.:

Synonyms:4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

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Technology Process of 4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

There total 1 articles about 4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2-(4-bromophenyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

: 73183-34-3
bis(pinacol)diborane

: 1104636-95-4
4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

Guidance literature:: With [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1021/acs.joc.5b00182

Reference yield:

: 1104636-95-4
4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

: 99770-93-1
benzene-1,4-diboronic acid bispinacol ester

Guidance literature:: 4-methyl-2,6-dioxo-8-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)hexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide; With potassium phosphate; In water; at 80 ℃; for 0.25h;

With Oxone; In water; at 70 ℃; for 1h; chemoselective reaction;
DOI:10.1039/C6SC04014D