dibenzyl pyrophosphate

Base Information

• Chemical Name: dibenzyl pyrophosphate
• CAS No.: 51478-53-6
• Molecular Formula: C₁₄H₁₆O₇P₂
• Molecular Weight: 358.224
• Mol file: 51478-53-6.mol

Synonyms:dibenzyl pyrophosphate

Chemical Property of dibenzyl pyrophosphate

Chemical Property:

Purity/Quality:

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Technology Process of dibenzyl pyrophosphate

There total 6 articles about dibenzyl pyrophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → phosphoric acid dibenzyl ester (1623-08-1) + dibenzyl pyrophosphate (51478-53-6)

Guidance literature:

With pyrophosphoric acid; triethylamine; trichloroacetonitrile; at 75 ℃; for 2h;

DOI:10.1246/bcsj.54.1891

Reference yield:

monobenzylphosphate (1623-07-0) + dicyclohexyl-carbodiimide (538-75-0) → dibenzyl pyrophosphate (51478-53-6)

Guidance literature:

With 1,4-dioxane; triethylamine; acetonitrile;

DOI:10.1021/ja01556a015

Reference yield:

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate (990-91-0) → dibenzyl pyrophosphate (51478-53-6)

Guidance literature:

With 2-ethoxy-ethanol; lithium chloride;

upstream raw materials:

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

amidophosphoric acid monobenzyl ester

monobenzylphosphate

dicyclohexyl-carbodiimide

Downstream raw materials:

monobenzylphosphate