1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

Base Information

Chemical Name:1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol
CAS No.:131157-72-7
Molecular Formula:C₅₄H₄₆O₁₅
Molecular Weight:934.95
Hs Code.:

Synonyms:1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

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Chemical Property of 1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

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Technology Process of 1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

There total 4 articles about 1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 131157-74-9
2,6-anhydro-3,4-di-O-benzoyl-1-deoxy-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-arabino-hex-1-enitol

: 131157-72-7
1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(90)80151-R

Reference yield:

: 131157-69-2
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranose

: 131157-72-7
1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / HBr / acetic acid / 5 h / Ambient temperature

2: 65 percent / sodium acetate, zinc dust, copper sulfate pentahydrate / H₂O; acetic acid / 3 h / -10 °C

3: 53 percent / H₂ / 33percent Pd-C / ethyl acetate / 16 h / Ambient temperature

With hydrogen bromide; hydrogen; sodium acetate; copper(II) sulfate; zinc; palladium on activated charcoal; In water; acetic acid; ethyl acetate;
DOI:10.1016/0008-6215(90)80151-R

Reference yield:

: 131157-70-5
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

: 131157-72-7
1,5-anhydro-3,4-di-O-benzoyl-6-deoxy-2-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / sodium acetate, zinc dust, copper sulfate pentahydrate / H₂O; acetic acid / 3 h / -10 °C

2: 53 percent / H₂ / 33percent Pd-C / ethyl acetate / 16 h / Ambient temperature

With hydrogen; sodium acetate; copper(II) sulfate; zinc; palladium on activated charcoal; In water; acetic acid; ethyl acetate;
DOI:10.1016/0008-6215(90)80151-R