1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

Base Information

Chemical Name:1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide
CAS No.:131157-70-5
Molecular Formula:C₆₁H₄₉BrO₁₇
Molecular Weight:1133.95
Hs Code.:

Synonyms:1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

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Chemical Property of 1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

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Technology Process of 1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

There total 2 articles about 1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 131157-69-2
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranose

: 131157-70-5
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 5h; Ambient temperature;
DOI:10.1016/0008-6215(90)80151-R

Reference yield:

: 98-88-4
benzoyl chloride

: 131157-70-5
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / pyridine / Ambient temperature

2: 86 percent / HBr / acetic acid / 5 h / Ambient temperature

With pyridine; hydrogen bromide; In acetic acid;
DOI:10.1016/0008-6215(90)80151-R

Reference yield: 65.0%

: 131157-70-5
1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-fructopyranosyl bromide

: 131157-74-9
2,6-anhydro-3,4-di-O-benzoyl-1-deoxy-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-D-arabino-hex-1-enitol

Guidance literature:: With sodium acetate; copper(II) sulfate; zinc; In water; acetic acid; at -10 ℃; for 3h;
DOI:10.1016/0008-6215(90)80151-R