4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

Base Information

Chemical Name:4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine
CAS No.:151266-28-3
Molecular Formula:C₂₄H₂₀IN₅O₅
Molecular Weight:585.358
Hs Code.:

Synonyms:4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

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Chemical Property of 4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

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Technology Process of 4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

There total 6 articles about 4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 151266-23-8
4-amino-3-iodo-1H-pyrazolo[3,4-d]pyrimidine

: 151378-79-9
methyl 5-deoxy-2,3-di-O-benzoyl-D-ribofuranoside

: 151266-28-3
4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

Guidance literature:: With boron trifluoride diethyl etherate; In nitromethane; for 1.5h; Heating;
DOI:10.1021/jm00074a024

Reference yield:

: 98-88-4
benzoyl chloride

: 151266-28-3
4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / pyridine / Ambient temperature

2: 88 percent / azobisisobutyronitrile (AIBN), HSnBu₃ / toluene / 2 h / 110 °C

3: 43 percent / BF₃*Et₂O / nitromethane / 1.5 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; In nitromethane; toluene;
DOI:10.1021/jm00074a024

Reference yield:

: 2380-63-4
4-Aminopyrazolo<3,4-d>pyrimidin

: 151266-28-3
4-amino-3-iodo-1-(2,3-di-O-benzoyl-5-deoxy-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / N-iodosuccinimide / dimethylformamide / 6 h / 80 °C

2: 43 percent / BF₃*Et₂O / nitromethane / 1.5 h / Heating

With N-iodo-succinimide; boron trifluoride diethyl etherate; In nitromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00074a024