(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

Base Information

Chemical Name:(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate
CAS No.:131938-97-1
Molecular Formula:C₁₈H₁₉NO₄
Molecular Weight:313.353
Hs Code.:

Synonyms:(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

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Chemical Property of (1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

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Technology Process of (1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

There total 1 articles about (1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 133725-55-0
(2S,3S)-5-methyl-3-(1-tosylindol-3-yl)cyclohex-4-ene-1,2-dicarboxylic acid anhydride

: 131938-97-1
(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In methanol; 1,2-dimethoxyethane; for 1.5h; Ambient temperature;

Reference yield:

: 131938-97-1
(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

: 131938-81-3
methyl 9-methyl-6-oxo-5-tosly-5,6,6aβ,7β,8,10aβ-hexahydroindeno<2,1-b>indole-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / PPE / CHCl₃ / 0.5 h / Heating

2: 1) TBAHS, aq. NaOH / 1) benzene, RT, 5 min, 2) benzene

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In chloroform;

Reference yield:

: 100-39-0
benzyl bromide

: 131938-97-1
(1RS,2SR,3SR)-1-methyl hydrogen 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

: 131939-07-6
(1RS,2SR,3SR)-2-benzyl 1-methyl 3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

: 131939-08-7
(1RS,2SR,3SR)-2-benzyl 1-methyl 3-(1'-benzylindol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylate

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; Yield given. Multistep reaction. Yields of byproduct given; 1) benzene, 0 deg C, 2) RT, 1 h;