(2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester]

Base Information

• Chemical Name: (2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester]
• CAS No.: 886844-43-5
• Molecular Formula: C₃₆H₃₅N₇O₅
• Molecular Weight: 645.718

Synonyms:(2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester]

Chemical Property of (2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester]

Chemical Property:

Purity/Quality:

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Technology Process of (2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester]

There total 1 articles about (2'R,4'R,7'S)-4'-(N⁶-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

(2'R,4'R)-4'-(N6-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinium chloride + (2R)-methyl 2-bromopropionate (20047-41-0) → (2'R,4'R,7'S)-4'-(N6-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester] (886844-43-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1039/b518171b

Reference yield:

(2'R,4'R,7'S)-4'-(N6-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid methyl ester] (886844-43-5) → (2'R,4'R,7'S)-4'-(N6-benzoyladenin-9-yl)-2'-[(fluoren-9-yl-methoxycarbonyl)aminomethyl]-pyrrolidinyl-N-[(α-methyl)acetic acid] hydrochloride

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / dioxane / 18 h / Heating

2: 270 mg / pyridine / 2 h / Heating

With pyridine; hydrogenchloride; In 1,4-dioxane;

DOI:10.1039/b518171b

upstream raw materials:

(2R)-methyl 2-bromopropionate

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