bis(acetylacetonato)chlorophenylzirconium

Base Information

Chemical Name:bis(acetylacetonato)chlorophenylzirconium
CAS No.:75780-56-2
Molecular Formula:C₃₂H₃₈Cl₂O₈Zr₂
Molecular Weight:804.003
Hs Code.:

Synonyms:bis(acetylacetonato)chlorophenylzirconium

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Chemical Property of bis(acetylacetonato)chlorophenylzirconium

Chemical Property:

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Technology Process of bis(acetylacetonato)chlorophenylzirconium

There total 3 articles about bis(acetylacetonato)chlorophenylzirconium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75763-81-4
bis(acetylacetonato)dichlorozirconium

: 587-85-9,1337-09-3
diphenylmercury(II)

: 75780-56-2
bis(acetylacetonato)chlorophenylzirconium

: 100-56-1
phenylmercury(II) chloride

Guidance literature:: In tetrahydrofuran; stirring (-10°C, 6 h); solvent removal (vac.), toluene addn., ppt. centrifuged off, crystn. (toluene/hexane);

Reference yield:

: 75763-81-4
bis(acetylacetonato)dichlorozirconium

: 75780-56-2
bis(acetylacetonato)chlorophenylzirconium

Guidance literature:: With phenylmagnesium bromide; In tetrahydrofuran; stirring (-40°C), warming to 0°C (10-12 h), pptn. of Mg-salts on dioxane addn.; solvent removal (vac.), toluene addn., ppt. centrifuged off, pptn. on hexane addn.; elem. anal.;

Reference yield:

: 75763-81-4
bis(acetylacetonato)dichlorozirconium

: 591-51-5
phenyllithium

: 75780-56-2
bis(acetylacetonato)chlorophenylzirconium

Guidance literature:: With phenylmagnesium bromide; In diethyl ether; mixing of solns (-78°C), warming to room temp.; solvent removal (vac.), toluene addn., ppt. centrifuged off, crystn. (toluene/hexane);