tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

Base Information

Chemical Name:tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate
CAS No.:1351304-91-0
Molecular Formula:C₃₇H₆₀N₈O₇
Molecular Weight:728.933
Hs Code.:

Synonyms:tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

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Chemical Property of tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

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Technology Process of tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

There total 1 articles about tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1093239-07-6
11-prop-2-ynyl-1,4,8,11-tetraaza-cyclotetradecane-1,4,8-tricarboxylic acid tri-tert-butyl ester

: 116433-53-5
2-azido-N-(phenylmethyl)acetamide

: 1351304-91-0
tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1021/ic2020012

Reference yield: 100.0%

: 1351304-91-0
tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

: 76-05-1
trifluoroacetic acid

: 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)-methyl)-11-aza-1,4,8-triazoniacyclotetradecane-1,4,8-triium tri-trifluoroacetate

Guidance literature:: In dichloromethane; water; at 20 ℃; for 6h;
DOI:10.1021/ic2020012

Reference yield:

: 1351304-91-0
tri-tert-butyl 11-((1-(2-(benzylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

: C₂₂H₃₄⁽²⁾H₂N₈O

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane; water / 6 h / 20 °C

2: potassium hydroxide / water / pH 11 - 12

3: d⁽⁴⁾-methanol

With d⁽⁴⁾-methanol; potassium hydroxide; In dichloromethane; water;
DOI:10.1021/ic2020012